TU-1901 plus闆欏厜鏉熺传澶栧彲瑕嬪垎鍏夊厜搴﹁▓
閰堕厷娣峰悎娑�:钁¤悇绯栨哀鍖栭叾(GOD)閬庢哀 鍖栫墿閰�(POD) 4-姘ㄥ熀瀹� 鏇垮悺鍟�(4-AAP)鑻厷(0.1%).妯�(bi膩o)婧�(zh菙n)钁¤悇绯栨憾娑�: 0.2mg/mL銆�
寰呮脯钁¤悇绯栨憾娑叉恫 (2)鍙嶆噳(y墨ng):娣峰嫽锛�37C淇濇韩20min,鍐疯嚦瀹ゆ韩; (3)娓噺:浠ョ┖鐧界瑾�(di脿o)闆�锛� 500nm娉㈤暦铏曟脯瀹氬悇绠″惛鍏夊害鍊�(鍙嶅京(f霉)璁�鏁�(sh霉)3娆�锛屽彇鍧囧��) (4)瑷堢畻:妯ｅ搧钁¤悇绯栧惈閲�(mg/mL) = A妯�/A妯�(bi膩o)X妯�(bi膩o)婧�(zh菙n)婧舵恫婵冨害銆�
鍦ㄤ笂杩拌│绠′腑鍒嗗垾鍔犲叆DNS瑭﹀姂2.0ml,浜庢哺姘存荡涓姞鐔�2min閫�(j矛n)琛岄’鑹�锛屽彇鍑哄悗鐢ㄦ祦鍕曟按杩呴�熷喎鍗�锛屽悇鍔犲叆鐕曢ぞ姘�9.0ml,鎼栧嬀锛屽湪540mm娉㈤暦铏曟脯瀹氬厜鍚告敹鍊笺�備互1.0ml鐕曢ぞ姘翠唬鏇胯憽钀勭硸妯�(bi膩o)婧�(zh菙n)娑叉寜鍚屾ǎ椤壊鎿嶄綔鐐虹┖鐧借(di脿o)闆堕粸銆備互钁¤悇绯栧惈閲�(mg)鐐烘┇鍧愭(bi膩o)锛屽厜鍚告敹鍊肩偤绺卞潗妯�(bi膩o)锛岀躬鍒舵(bi膩o)婧�(zh菙n)鏇茬窔銆�
妯ｅ搧涓倓鍘熺硸鐨勬彁鏀�
婧�(zh菙n)纰虹ū鍙�0.5g 妫茬矇锛屾斁鍦�100ml鐕掓澂涓紝鍏堜互灏戦噺钂搁ぞ姘�(绱�2 m)瑾�(di脿o)鎴愮硦鐙�锛岀劧鍚庡姞鍏�40ml钂搁ぞ姘达紝娣峰嫽锛屼簬50C鎭掓韩姘存荡涓繚婧�20min,涓嶆檪鏀媽锛屼娇閭勫師绯栨蹈鍑烘贩銆傞亷婵�锛屽皣婵炬恫鍏ㄩ儴鏀堕泦鍦�50ml鐨勫閲忕摱涓紝鐢ㄨ捀椁炬按瀹氬鍏ㄥ埢搴�锛屽嵆鐐洪倓鍘熺硸鎻愬彇娑层��
1.妯ｅ搧绺界硸鐨勬按瑙ｅ強鎻愬彇
婧�(zh菙n)纰虹ū鍙�0.5g鐜夌背娣�绮�锛屾斁鍦ㄩ寪褰㈢摱涓�锛屽姞鍏�6mol/L HCI 10ml,鐕曢ぞ姘�15ml,鍦ㄦ哺姘存礇涓姞鐔�0.5h.鍙栧嚭1~2婊寸疆浜庣櫧鐡锋澘涓�锛屽姞1婊�1-KI婧舵恫妾㈡煡姘磋В瓒冲惁瀹屽叏銆傚宸叉按瑙�? 瀹屽��锛屽墖涓嶆棭鐝�(xi脿n)钘�(l谩n)鑹�銆傛按瑙ｇ暍锛� 鍐峰嵒鑷冲婧悗鍔犲叆1婊撮殠閰炴寚绀哄姂锛屼互6N NaOH婧舵恫涓拰鍊嬫荡娑插憟寰磪鑹�锛屽苟瀹氬鍒�100m閬庢烤鍙栨烤娑�10ml浜�100ml瀹归噺鐡朵腑锛屼綘瀹瑰叏鍒诲害锛屾贩缈�(x铆)锛屽嵆鐐虹█閲�1000鍊嶇殑绺界硸姘磋В娑诧紝鐢ㄤ簬绺界硸娓畾銆�
鍥涖�佹ǎ鍝佷腑鍚瀽閲忕殑娓畾
鍙�7鏂�15mmx 180mm瑭︾锛屽垎鍒ユ寜涓嬮暦鍔犲叆瑭﹀姂:
